Calcium stearate is carboxylate of calcium, classified as a calcium soap. It is a component of some lubricants, surfactants, as well as many foodstuffs. It is a white waxy powder.
Practically insoluble in water, ether, chloroform, acetone; slightly soluble in ethanol (95%).
IP/BP/EP/USP
3.
Identification
(A) Gives the test for calcium
(B) Congealing temperature: Not below 540 C.
(C) The residue has a freezing point not lower than 53 °C.
(D) The acid value of the fatty acids is 195 to 210
(A) IP/BP/EP/USP (B) IP/BP/EP (C) & (D) BP/EP
4.
Acidity Or Alkalinity
NMT0.5 ml of 0.01 M hydrochloric acid or 0.01 M sodium hydroxide is required to change the colour of the indicator.
BP/EP
5.
Composition Of Fatty Acid
To comply the test by gas chromatography.
IP/BP/EP/USP
6.
Chlorides
Maximum 0.1% w/w.
BP/EP
7.
Sulfates
Maximum 0.3% w/w.
BP/EP
8.
Cadmium
Maximum 3 ppm . (Atomic absorption spectrometry)
BP/EP
9.
Lead
Maximum 10 ppm (Atomic absorption spectrometry)
BP/EP
10.
Nickel
Maximum 5 ppm. (Atomic absorption spectrometry)
BP/EP
11.
Microbial Contamination
(A) Total aerobic microbial count: Maximum 1000 cfu/g.
(B) Total yeast and mould count : Maximum 100 cfu/g
(C) Escherichia coli & Salmonella: Should be absent.
BP/EP
12.
Loss On Drying
(A) Not more than 4.0% w/w at 105 Celcius
(B) Not more than 6.0% w/w at 105 Celcius
(A) IP/USP (B) BP/EP
13.
Heavy Metals
Not more than 10 ppm.
IP/USP
14.
Assay
(A) Calcium Stearate
(B) Fatty Acid
Composition:
(1) Stearic Acid
(2) Sum Of Stearic Acid & Palmitic Acid
(A) Between 9.0 % w/w. to 10.5 % w/w of ‘CaO’, .
(B) Between 6.4% to 7.4%w/w.
(1) Minimum 40.0% w/w.
(2) Minimum 90.0% w/w.